滕州市浩瀚色谱仪器技术服务有限公司
主营产品:气相色谱仪,液相色谱仪,色谱柱,顶空进样器,热解析仪,水分测定仪,分光光度计
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产品名称: 苯中微量噻吩测定专用毛细管柱 HH-SF-II
产品编号: 20170256987
产品商标: 浩瀚色谱
产品规格: HH-SF-II
参考价格: 面议
更新日期: 2024/4/28 11:20:00
被阅次数: 330次
 
  • 详细说明
   苯加氢工艺所用原料粗苯中的硫化物主要有噻吩、二硫化碳等,硫化物杂质通过加氢后转化为相应的烷烃及硫化氢,再通过环丁砜萃取蒸馏工艺除去非芳烃杂质。尽管脱硫反应有很高的化学平衡转化率,但脱硫率并不一定很高。
   滕州市浩瀚色谱仪器技术服务有限公司,研发出HH-SF-II专用毛细管柱,建立了超高灵敏度气相色谱仪测定苯中微量噻吩的方法,对色谱条件进行了优化,定量方法采用外标法。该方法的加标回收率为114%~136%;相对标准偏差(RSD)不大于7%。测定苯样品中微量噻吩具有灵敏度高、重现性好和可靠性高等优点。



Benzene hydrogenation process used in crude benzene sulfide mainly thiophene, carbon disulfide, sulfide impurities through hydrogenation into the corresponding alkane and hydrogen sulfide, and then through the sulfolane extraction distillation process to remove non-aromatic impurities. Although the desulfurization reaction has a high chemical conversion rate, but the desulfurization rate is not necessarily high.
    The HH-SF-II capillary column was developed and the ultra-high sensitivity gas chromatograph was used to determine the amount of thiophene in benzene. The chromatographic conditions were optimized and quantified by external standard method. The The recoveries of the method were 114% ~ 136% and the relative standard deviations (RSDs) were less than 7%. The determination of trace thiophenes in benzene samples has the advantages of high sensitivity, good reproducibility and high reliability.
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